Hawthorn Pills

山楂化滞丸【Prescription】 Hawthorn 500g Malt 100g Liushen 100g
Betel nut 50g Laizizi 50g, beef, 50g
【Method】 The above six flavors are pulverized into fine powder, sieved and mixed. Add brown sugar 25g and refined honey 90g per 100g powder
~100g made into a big honey pill, that is.
【Properties】 This product is brown big honey pill; tastes sour and sweet.
[Identification] (1) Take this product and observe under the microscope: the pericarp cells are pale purple, red or yellowish brown.
It is round or polygonal in shape and has a diameter of about 125 μm. In the column of pericarp cells, there is often one long cell connected to two short cells, and the long cell wall is thick, wavy and woody. The endosperm fragments are colorless, the walls are thicker, and there are more large rounded holes. The seed coat cells are light brown or brown, 48 to 80 μm long. The seed coat fragments are yellow or brownish red, with small cells, polygonal shapes and wall thickness.
(2) Take 9g of this product, add appropriate amount of diatomaceous earth, stir well, add 50ml of methanol, reflux on water bath for 30 minutes, filter.
Take 2ml of the filtrate, add 2 drops of cesium iodide test solution to form a reddish brown precipitate; take another 2ml of filtrate, add 2 drops of silicotungstic acid test solution,
A white precipitate formed.
(3) Take the filtrate under [Identification] (2) as the test solution. Another ursolic acid reference substance was added, and methanol was added to make a solution containing 1 mg per 1 ml as a reference solution. According to the thin layer chromatography (Appendix VI B) test, 10 μl of each of the above two solutions was aspirated and placed on the same silica gel G thin layer plate with sodium carboxymethyl cellulose as the binder, with chloroform-acetone (9: 1) As a developing agent, unroll, take out, dry, spray with 10% sulfuric acid in ethanol, and bake at 105 ° C for several minutes. In the chromatogram of the test sample, spots of the same color are displayed at positions corresponding to the chromatogram of the reference substance.
[Check] It should comply with the relevant provisions under the pill (Appendix I A).
【Functions and Indications】 Digestive stagnation. It is used to stop eating and stagnate, eat less and stay in the stool, constipation, and fullness.
[Usage and Usage] Oral, 2 pills a day, 1 or 2 times a day.
【Note】 Pregnant women should not take it.
[Specifications] Each pill weighs 9g
[Storage] Sealed.

Sunitinib Intermediates

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